![]() | Lunar rocks and regolith returned by the Apollo missions |
![]() | Meteorites recovered by the U.S. Antarctic Search for Meteorites |
![]() | Dust particles collected from the stratosphere |
![]() | Space-exposed surfaces retrieved from satellites or spacecraft |
Maintaining samples in a pure state is critical to extracting scientific information from these unique, and often very small, samples. Equally important, however, is making the collection available for scientific study and education, because it is these activities that give the samples their true value. It is also wise to reserve portions of samples for future studies that will become possible with new or improved ideas and techniques.
Much of the research done on extraterrestrial samples involves measuring very small differences in composition; even tiny amounts of Earth materials can contaminate and ruin scientific measurements. Contamination could be caused by airborne particles getting into the sample or by reaction of the sample with the Earth's atmosphere.
Examples:
The amount of lead in a solder droplet exceeds the amount of lead in all 382 kilograms of lunar samples. It happens that lead resulting from radioactive decay of uranium is one of the indicators used to measure the age of rocks; thus, any Earth-based lead is common in many electrical devices routinely used in laboratories but must be carefully avoided during sample curation.
Moon soil contains pure iron metal, which would quickly rust in Earth's atmosphere, and water-free glass, which reacts with moisture to form clays. Samples must be kept under inert gas.
Our various curatorial laboratories deal with contamination in slightly different ways. Generally, airborne particulate contamination is controlled by air filtration, special clothing on personnel, restricting the types of materials that are used in the laboratory for tools and containers, and scrupulously cleaning the tools and containers that touch the samples. A special team of technicians cleans and certifies tools used in the laboratories. To keep samples from reacting with the Earth's atmosphere, samples are enclosed in gloved cabinets filled with pure nitrogen.
In addition to purely scientific information, accounting data, such as sample location or weight is also recorded. The curators know where the samples are and how they are being used. Computer data bases are updated daily based on work done in curatorial laboratories and information received from scientific investigators.
Newly obtained samples are examined and classified, so that scientists can use the samples appropriately. For large samples, such as lunar and meteorite samples, examination may consist of observation through the binocular microscope and the preparation of a thin section, from which mineral composition can be identified. For samples too small to see with ordinary means, such as cosmic dust and space-dust impact craters, additional examination may be done with a scanning electron microscope which reveals the particle shape and chemical composition. For some samples, such as the remaining unopened lunar soil cores, the opening, careful dissection and description may take months.
The curatorial staff plans to build on past experience in preparing for the technological challenges of the future. Anticipated challenges include improvements in materials used to touch samples, container seals, manipulation and storage of samples at low temperature and low pressure, cost effieiencies in managing the samples, and rapid, innovative distribution of samples and sample information to scientists and educators. Rocks, soil and ices from Mars and comets pose special challenges to collect, transport, store and study under their natural environmental conditions of extremely low temperatures and pressures. For comets, temperatures of 130 K (-226 F) and vacuum conditions may be appropriate; for Mars 230 K ( -46 F) and a pressure equal to only 1% of Earth's may be required. Future samples may come from: Moon, Mars, Space Station Cosmic Dust Collection Facility, Space-exposed hardware, comets, asteroids, other stratospheric dust samples such as volcanic ash, and special Earth samples.